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The first comprehensive analysis of the flavor of Freekeh: a toasted, smoked, green durum wheat product, by analytical and sensory approaches

Cna'ani, Alon; Scharling, Eva; Hjerrild, Sabrina Krogh; Li, Qian; Sárossy, Zsuzsa; Wrona, Magdalena; Pauly, Markus; Rinnan, Åsmund; Lametsch, Rene; Nerin, Cristina and Frøst, Michael Bom (2026) The first comprehensive analysis of the flavor of Freekeh: a toasted, smoked, green durum wheat product, by analytical and sensory approaches. Food Chemistry, 532 (151571), pp. 1-23.

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Summary

Freekeh, smoked immature durum wheat, has gastronomic significance and attractive nutritional values, fueling increasing global demand. Yet, knowledge regarding its flavor chemistry and sensory properties remains absent, hindering quality control and market expansion. We employed analytical and sensory methods, with multivariate modeling, to study how Freekeh flavor is shaped by agro-technical and processing practices. Freekeh flavor is a mixture of grain-derived metabolites and processing products, yielding >300 volatiles. Twenty volatiles were validated as key-odorants (phenols, pyrazines, aldehydes) via GC-olfactometry; phenols comprising most of the profile. Grain maturity significantly influences flavor: early-harvest Freekeh is more aromatic, sweet, umami and kokumi due to elevated sugars, amino acids, 5’-ribonucleotides and γ-glutamyl peptides. Genotype and toasting intensity similarly play a pivotal role in shaping flavor. This study serves as the inaugural roadmap to freekeh flavor, establishing a predictive chemical/sensory framework uncovering novel cereal flavors, and providing producers benchmarks to fine-tune quality using early-harvest practices.


EPrint Type:Journal paper
Keywords:Wheat, Flavor, Durum, Freekeh, GCMS, grain
Agrovoc keywords:
Language
Value
URI
English
wheat
http://aims.fao.org/aos/agrovoc/c_8373
English
flavor -> flavour
http://aims.fao.org/aos/agrovoc/c_10893
English
durum (Triticum durum) -> hard wheat
http://aims.fao.org/aos/agrovoc/c_11456
English
grain
http://aims.fao.org/aos/agrovoc/c_3346
Subjects: Food systems > Processing, packaging and transportation
Research affiliation: Denmark > ICROFS - International Centre for Research in Organic Food Systems
Denmark > KU - University of Copenhagen
Denmark > Organic RDD 7 > BOOST
Horizon Europe or H2020 Grant Agreement Number:893818
ISSN:1873-7072
DOI:10.1016/j.foodchem.2026.151571
Deposited By: Frøst, PhD Michael Bom
ID Code:58253
Deposited On:06 Nov 2026 11:13
Last Modified:06 Nov 2026 11:13
Document Language:English
Status:Published
Refereed:Peer-reviewed and accepted
Additional Publishing Information:This is the final article published in Food Chemistry

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